Description
Metal-organic Frameworks in Analytical Sample Preparation and Sensing presents all the areas of applications of metal-organic frameworks in analytical sample preparation. Metal-organic frameworks are crystalline coordination polymers with robust and stable crystal structures, high synthetic tunability, and interesting properties for their use in analytical applications, including their detailed use as sorbents in miniaturized-extraction procedures and as components in sensors.This book also provides important information about the synthesis and characterization of these materials, with useful tips written by experts on the subject with respect to their conditioning, handling, and recycling. Their outstanding properties, adsorptive capabilities, and structural diversity are also highlighted. This will help experts in the field to select the proper metal-organic framework for a particular analytical application.- Provides analytical scientists with a unified reference guide for the use of metal-organic frameworks in miniaturized-extraction methods and sensing.- Covers aspects related to the development, characterization, conditioning and handling of metal-organic frameworks. Issues of scale-up will be covered too.- Addresses the proper metal-organic framework for a particular analytical miniaturized method.
Table of Contents
Section 1: Reticular materials: synthesis, characterization, and properties1. Introduction and general aspects of metal-organic frameworks and other novel reticular materials2. Synthesis of metal-organic frameworks with interest in analytical chemistry3. Synthesis of covalent-organic frameworks with interest in analytical chemistry4. Synthesis of composites based on reticular materials with interest in analytical chemistrySection 2: Metal-organic frameworks as sorbents in analytical sample preparation5. Metal-organic frameworks in micro-solid phase extraction6. Metal-organic frameworks in micro-dispersive solid phase extraction and stir bar sorptive extraction7. Metal-organic frameworks in magnetic-based methods8. Metal-organic frameworks in solid-phase microextractionIncludes both in-fiber and in-tube solid-phase microextraction9. Metal-organic frameworks in thin film microextraction10. Hyphenating microextraction methods based on metal-organic frameworks with chromatographic techniquesSection 3: Metal-organic frameworks as sensors for analysis11. Metal-organic frameworks as luminescence sensors12. Metal-organic frameworks as electrochemical sensors13. Other sensing applications of metal-organic frameworksSection 4: Novel reticular materials in analytical sample preparation and sensing14. Covalent-organic frameworks in sample preparation15. Covalent-organic frameworks as sensors for analysis
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