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基本説明
For the first time, this comprehensive handbook presents the emerging field of microwave technology for the synthesis of nanoparticles.
Full Description
For the first time, this comprehensive handbook presents the emerging field of microwave technology for the synthesis of nanoparticles. Divided into three parts--fundamentals, methods, and applications--it covers topics including microwave theory, scale-up, microwave plasma synthesis, characterization, and more. This offers both an important volume for academic researchers, and a resource for those in industry exploring the applications of nanoparticles in semiconductors, electronics, catalysis, sensors, and more.
Contents
PREFACE
INTRODUCTION TO NANOPARTICLES
General Introduction to Nanoparticles
Methods of Nanoparticle Synthesis
Surface Plasmon Resonance and Coloring
Control of Size, Shape, and Structure
Reducing Agent in Nanoparticle Synthesis
Applications of Metallic Nanoparticles
GENERAL FEATURES OF MICROWAVE CHEMISTRY
Microwave Heating
Some Applications of Microwave Heating
Microwave Chemistry
Microwave Chemical Reaction Equipment
CONSIDERATIONS OF MICROWAVE HEATING
General Considerations of Microwave Heating
Peculiar Microwave Heating
Relevant Points of Effective Microwave Heating
COMBINED ENERGY SOURCES IN THE SYNTHESIS OF NANOMATERIALS
Introduction
Simultaneous Ultrasound/Microwave Treatments
Sequential Ultrasound and Microwaves
Conclusions
NANOPARTICLE SYNTHESIS THROUGH MICROWAVE HEATING
Introduction
Microwave Frequency Effects
Nanoparticle Synthesis under a Microwave Magnetic Field
Synthesis of Metal Nanoparticles by a Greener Microwave Hydrothermal Method
Nanoparticle Synthesis with Microwaves under Cooling Conditions
Positive Aspects of Microwaves - Thermal Distribution in Nanoparticle Synthesis
Microwave-Assisted Nanoparticle Synthesis in Continuous Flow Apparatuses
MICROWAVE-ASSISTED SOLUTION SYNTHESIS OF NANOMATERIALS
Introduction
Synthesis of ZnO Nanocrystals
Synthesis of a-Fe2O3 Nanostructures
Element-Based Nanostructures and Nanocomposite
Chalcogenide Nanostructures
Graphene
Summary
PRECISELY CONTROLLED SYNTHESIS OF METAL NANOPARTICLES UNDER MICROWAVE
IRRADIATION
Introduction
Precise Control of Single Component under Microwave Irradiation
Precise Control of Multicomponent Structures under Microwave Irradiation
An Example of Mass Production Oriented to Application
Conclusion
MICROWAVE-ASSISTED NONAQUEOUS ROUTES TO METAL OXIDE NANOPARTICLES
AND NANOSTRUCTURES
Introduction
Nonaqueous Sol -
Gel Chemistry
Polyol Route
Benzyl Alcohol Route
Other Mono-Alcohols
Ionic Liquids
Nonaqueous Microwave Chemistry beyond Metal Oxides
Summary and Outlook
INPUT OF MICROWAVES FOR NANOCRYSTAL SYNTHESIS AND SURFACE
FUNCTIONALIZATION FOCUS ON IRON OXIDE NANOPARTICLES
Introduction
Biomedical Applications of Iron Oxide Nanoparticles
Nanoparticle Synthesis
Nanoparticle Surface Functionalization
Microwave-Assisted Chemistry
Conclusions
MICROWAVE-ASSISTED CONTINUOUS SYNTHESIS OF INORGANIC NANOMATERIALS
Introduction and Overview
Microwave-Assisted Continuous Synthesis of Inorganic Nanomaterials
Types of Microwave Apparatus Used in Continuous Synthesis
Microwave Continuous Synthesis of Molecular Sieve Materials
Microwave Continuous Synthesis of Metal Oxides and Mixed Metal Oxide Materials
Microwave Continuous Synthesis of Metallic Nanomaterials
Conclusions and Outlook
MICROWAVE PLASMA SYNTHESIS OF NANOPARTICLES: FROM THEORETICAL BACKGROUND AND EXPERIMENTAL REALIZATION TO NANOPARTICLES WITH SPECIAL PROPERTIES
Introduction
Using Microwave Plasmas for Nanoparticle Synthesis
Experimental Realization of the Microwave Plasma Synthesis
Infl uence of Experimental Parameters
Nanoparticle Properties and Application
Summary
OXIDATION, PURIFI CATION AND FUNCTIONALIZATION OF CARBON NANOTUBES UNDER
MICROWAVE IRRADIATION
Introduction
Oxidation and Purifi cation
Functionalization
Conclusion
INDEX
