Practical Microwave Synthesis for Organic Chemists : Stategies, Instruments, and Protocols （2008. VIII, 296 p. 24 cm）

Kappe, C. Oliver/ Dallinger, Doris/ Murphree, Shaun

WILEY-VCH（2008発売）

• 製本 Hardcover:ハードカバー版／ページ数 297 p.
• 商品コード 9783527320974

Full Description

With the novice user in mind, this beginner's guide explains the basics behind microwave technology, evaluates available instruments and reaction modes, and provides practical hints for every eventuality. Includes 27 detailed protocols for often-used reactions. From the contents:
1 Microwave Synthesis - An Introduction
2 Microwave Theory
3 Equipment Review
4 Microwave Processing Techniques
5 Starting With Microwave Chemistry
6 Experimental Protocols
6.1 General Small-Scale Sealed-Vessel Microwave Processing
6.2 Reaction Optimization
6.3 Library Generation
6.4 Reaction Scale-Up
6.5 Special Processing Techniques

Contents

1 Microwave Synthesis -
An Introduction 1
2 Microwave Theory 11
3 Equipment Review 45
4 Microwave Processing Techniques 87
5 Starting With Microwave Chemistry 163
6 Experimental Protocols 205
6.1 General Small-Scale Sealed-Vessel Microwave Processing 207
6.2 Reaction Optimization 234
6.3 Library Generation 239
6.4 Reaction Scale-Up 251
6.5 Special Processing Techniques