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Full Description
Because of its simplicity of use and quantitative results, Scanning Electrochemical Microscopy (SECM) has become an indispensable tool for the study of surface reactivity. The fast expansion of the SECM field during the last several years has been fueled by the introduction of new probes, commercially available instrumentation, and new practical applications. Scanning Electrochemical Microscopy, Second Edition offers essential background and in-depth overviews of specific applications in self-contained chapters.
Recent methodological advances have greatly increased the capacity of SECM to characterize interfaces at the nanoscale and to obtain molecular-level chemical information. This thoroughly updated edition retains original chapters describing the principles of SECM measurements, instrumentation, preparation of SECM probes, imaging methodologies, and theory and offers:
New chapters on studies of single biological cells, corrosion, electrocatalysis, and hybrid techniques
Descriptions of recent advances of SECM in several areas of current interest: biotechnological applications, nanofabrication and surface patterning, and molecular transport across films and membranes
Discussion of the ongoing shift from micrometer-scale experiments to the nanoscale
Useful for a broad range of interdisciplinary research—from biological systems to probing reactions at the liquid-liquid interface—this book is invaluable to all interested in learning and applying SECM.
Contents
Introduction and Principles. Instrumentation. Preparation of Tips for Scanning Electrochemical Microscopy. Scanning Electrochemical Microscopic Imaging. Theory. Heterogeneous Electron Transfer Reactions. Visualizing and Quantifying Homogeneous Chemical Reactions in Electrochemical Processes. Charge Transfer Processes at the Liquid-Liquid Interface. Imaging Molecular Transport across Membranes. Potentiometric Probes. Biotechnological Applications. Scanning Electrochemical Microscopy of Living Cells. Localized Flux Measurements and Kinetic Imaging at Interfaces. Applications of Scanning Electrochemical Microscopy in Corrosion Research. Micro- and Nanopatterning Using Scanning Electrochemical Microscopy. Application to Electrocatalysis and Photocatalysis and Surface Interrogation. Hybrid Scanning Electrochemical Techniques: Methods and Applications. Additional Recent Applications and Prospects. Index.
