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Full Description
The current volume continues the tradition of providing significant and interesting procedures, which should prove worthwhile to many synthetic chemists working in increasingly diverse areas. Following precedent, there is no specific or central theme to this volume.
Contents
Preparation of (3,5-Dimethoxy-1-Phenyl Cyclohexa-2,5-Dienyl)-Acetonitrile Through Birch Reductive Alkylation (BRA) (Raphael Lebeuf, Muriel Berlande, Frédéric Robert, and Yannick Landais). Synthesis of Tert-Butyl (1S,2S)-2-Methyl-3-Oxo-1-Phenylpropylcarbamate By Asymmetric Mannich Reaction (Jung Woon Yang, Subhas Chandra, Pan, and Benjamin List).
Synthesis of Pyrazolo[1,5-a]Pyridines Via Azirines: Preparation of 2-(3-Bromophenyl)-6-(Trifluoromethyl)Pyrazolo[1,5-a]Pyridine (Stephen Greszler and Kirk L. Stevens).
Benzyl Alcohol as an Alkylating Agent Using the Ruthenium-Catalyzed Borrowing Hydrogen Strategy (Tracy D. Nixon, Paul A. Slatford, Michael K. Whittlesey and Jonathan M. J. Williams).
2-(2,2-Dibromoethenyl)-Benzenamine (Christopher Bryan, Valentina Aurregi and Mark Lautens).
(S)-(-)-2-Allylcyclohexanone (Manfred Braun, Panos Meletis, and Mesut Fidan).
Preparation of 4-Spirocyclohexyloxazolidinone By C-H Bond Nitrene Insertion (Kim Huard and Hélène Lebel).
Preparation of (S)-4-Isopropyl-N-Propanoyl-1,3-Thiazolidine-2-Thione (Erik Gálvez, Pedro Romea, and Felix Urpi).
Stereoselective Synthesis of Anti α-Methyl-ß-Methoxy Carboxylic Compounds (Erik Gálvez, Pedro Romea, and Fèlix Urpi).
Synthesis of 2-Arylindole-4-Carboxylic Amides: [2-(4-Fluorophenyl)-1H-Indol-4-YL]-1-Pyrrolidinylmethanone (Jeffrey T. Kuethe and Gregory L. Beutner).
Palladium (II) Acetate-Butyldi-1- Adamantylphosphine Catalyzed Arylation of Electron-Rich Heterocycles. Preparation of 5-Phenyl-2-Isobutylthiazole (Anna Lazareva, Hendrich A. Chiong, and Olafs Daugulis).
Mild and Efficient One-Pot Curtius Rearrangement: Preparatino of N-Tert-Butyl Adamantanyl-1-YL-Carbamate (Olivier Leogane and Hélène Lebel).
Enantioselective Oxidation of An Alkyl Aryl Sulfide: Synthesis of (S)-(-) Methyl p-Bromophenyl Sulfoxide (Carmelo Drago, Emma-Hane Walker, Lorenzo Caggiano and Richard F. W. Jackson).
Protection of Diols with 4-(tert-Butyldimethylsilyloxy)Benzylidene Acetal and Its Deprotection:(4-((4R,5R)-4,5-Diphenyl-1,3-Dioxolan-2-YL) Phenoxy) (Tert-Butyl)Dimethylsilane (Hiroyuki Osajima, Hideto Fujiwara, Kentaro Okano, Hidetoshi Tokuyama, and Tohru Fukuyama).
Synthesis of 2-[3,3'-DI-(Tert-Butoxycarbonyl)-Aminodipropylamine]-4,6,-Dichloro-1,3,5-[Tris-Piperazine]-Triazine As a Core for the Large Scale Syntehsis of Melamine (Triazine) Dendrimers (Abdellatif Chouai, Vincent J. Venditto, and Eric E. Simanek).
Large Scale, Green Syntehsis of a Generation-1 Melamine (Triazine) Dendrimer) (Abdellatif Chouai, Vincent J. Venditto, and Eric E. Simanek).
The Direct Acyl-Alkylation of Arynes. Preparation of Methyl 2-(2-Acetylphenyl) Acetate (David C. Ebner, Uttam K. Tambar, and Brian M. Stoltz).
Convenient Preparation of 3-Ethoxycarbonyl Benzofurans From Salicylaldehydes adn Ethyl Diazoacetate (Matthew E. Dudley, M. Monzur Morshed, and M. Mahmun Hossain).
Preparation of (S)-Tert-Butylphon (Michael R. Krout, Justin T. Mohr, and Brian M. Stoltz).
Preparation of (S)-2-Allyl-2-Methylcyclohexanone (Justin T. Mohr, Michael R. Krout, and Brian M. Stoltz).
Phosphine-Catalyzed [4+2] Annulation: Synthesis of Ethyl 6-Phenyl-1-Tosyl-1,2,5,6-Tetrahydropyridine-3-Carboxylate (Kui Lu and Ohyun Kwon).
Syntehsis of Polyynes by In Situ Desilylative Brominatino and Palladium-Catalyzed Coupling: (7-(Benzyloxy)Hepta-1,3,5-Triynyl) Triisopropylsilane (Soonho Hwang, Hee Ryong Kang, and Sanghee Kim).
Enantioselective Preparation of Dihydropyrimidones (Jennifer M. Goss, Peng Dai, Sha Lou, and Scott E. Schaus).
One-Pot Multicomponent Preparation of Tetrahydropyrzaoloquinolinones and Tetrahydropyrazoloquinazolinones (Toma N. Glasnov and C. Oliver Kape).
(3R,7aS)-3-(Trichloromethyl)Tetrahydropyrrolo[1,2-C]Oxazol-1(3H)-One: An Air and Moisture Stable Reagent For the Synthesis of Optically Active α-Branched Prolines (Gareld D. Artmann III, Ryan J. Rafferty, and Rovert M. Williams).
Vinylation with Inexpensive Silicon-Based Reagents: Preparation of 3-Vinylquinoline and 4-Vinylbenzophenone (Scott E. Denmark and Christophe R. Butler).
Low Pressure Carbonylation of Epoxides to ß-Lactones (John W. Kramer, Daniel S. Treitler, and Geoffrey W. Coates).
Tetrakis(Dimethylamino)Allene (Alois Fürstner, Manuel Alcarazo, and Helga Krause).
Efficient One-Pot Synthesis of Bis(4-Tert-Butylphenyl)Iodonium Triflate (Marcin Bielawski and Berit Olofsson).
Pd(0)-Catalyzed Diamination of Trans-1-Phenyl-1,3-Butadiene with Di-Tert-butyldiaziridinone As Nitrogen Source (Haifeng Du, Baoguo Zhao, and Yian Shi).
Synthesis of Ethyl 2-Ethanoyl-2-Methyl-3-Phenylbut-3-Enoate (Taisuke Fujimoto, Kohei Endo, Masaharu Nakamura, and Eiichi Nakamura).
Synthesis of 4,5-Dimethyl-1,3-Dithiol-2-One (Perumalreddy Chandreasekaran and James P. Donahue).
B-Protected Haloboronic Acids For Iterative Cross-Coupling (Steven G. Ballmer, Eric P. Gillis, and Martin D. Burke).
Rhodium-Catalyzed Enantioselective Addition of Arylboronic Acids to In Situ Generated N-Boc Arylimines. Preparatin of (S)-Tert-Butyl (4-Chlorophenyl) (Thiophen-2-YL)Methylcarbamate (Morten Storgaard and Jonathan A. Ellman).
Magnesiation of Weakly Activated Arenes Using tmp2Mg 2LiC1:Synthesis of Tert-Butyl Ethyl Phthalate (Christoph J. Rohbogner, Andreas J. Wagner, Giuliano C. Clososki, and Paul Knochel).
ERRATA.
1,4-BIS(Trimethylsilyl)Buta-1,3-Diyne (Graham E. Jones, David A. Kendrick, and Andrew B. Holmes).
