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Full Description
The volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested.
Contents
Preface. Notice to Contributors.Chapter One Metal Nitrosyl Complexes.1 Tetranitrosylchromium and Carbonyltrinitrosylmanganese.2 Dithiocarbamate Complexes of Iron and Cobalt Nitrosyls.3 Ammine Complexes of Osmium, Including Amminenitrosyls.4 Nitrosylammineruthenium Complexes.5 Dinitrosylcobalt Complexes.6 Bis(triphenylphosphine)chlorodinitrosylruthenium(1+)Tetrafluoroborate.7 Dicarbonyl-?-cyclopentadienylnitrosylmolybdenumand Bis(dihalo-?- cyclopentadienylnitrosylmolybdenum)Derivatives.8 Bis(methyldiphenylphosphine)dichloronitrosylcobalt.9 Tris(triphenylphosphine)nitrosylcobalt andTris(triphenylphosphine)nitrosylrhodium.10 Carbonylchloronitrosylrhenium Compounds.11 Decacarbonyldi-?-nitrosyl-trimetal Compounds.12 trans-Bis(triphenylphosphine)chloronitrosyliridium(1+)Tetrafluoroborate.Chapter Two Metal Carbonyl Compounds.13 Dodecacarbonyltriruthenium.14 Dodecacarbonyltriruthenium.15 Hexadecacarbonylhexarhodium.16Di-?-chloro-bis[tricarbonylchlororuthenium(II)].17Dicarbonyl(?-cyclopentadienyl)(thiocarbonyl)manganese(I).18 Transition Metal Carbonyl Derivatives of Magnesium.19 Tris(pentacarbonylmanganese)thalium(III).20 (Alkylamino)difluorophosphine- andHalodifluorophosphinetetracarbonyliron Complexes.21 Tris[bis(2-methoxyethyl)ether]potassium andTetraphenylarsonium Hexacarbonylmetallates(1?) of Niobium andTantalum.Chapter Three Werner Type Metal Complexes.22 (Dinitrogen oxide)pentaammineruthenium(II) Salts.23 Tetrakis(isothiocyanato)bis(2.2'-bipyridine)niobium(IV).24 Malonato Complexes of Chromium(III).25 Selenoureametal Complexes.26 Nickel Tetrafluorooxovanadate(IV) Heptahydrate.27 Polymeric Chromium(III)-bis(phosphinates).28 Resolution of thecis-Bromoamminebis(ethylenediamine)cobalt(III) Ion.29 Bis(alkylphosphine)trichlorotitanium(III) Complexes.Chapter Four Other Transition Metal Complexes.30 Reagents for the Synthesis of ?-Diene Complexesof Tricarbonyliron and Tricarbonylruthenium.31 Bis(?)-cyclopentadienylniobium Complexes.32 Dichloro(1,3-propanediyl)platinum andtrans-Dicholorobis(pyridine)(1,3-propane-diyl)platinumDerivatives.33 Olefin(?)silver(I) Compounds.34 Trichloromethyltitanium and Tribromomethyltitanium.35 Ethylenebis(triphenylphosphine)palladium(0) and RelatedComplexes.Chapter Five Main-Group and Actinide Compounds.36 Tetraethylammonium, Tetraphenylarsonium, and AmmoniumCyanates and Cyanides.37 Diindenylmagnesium.38 Fluoromethylsilanes.39 Uranium Hexachloride.40 Cholorotris(?-cyclopentadienyl) Complexes ofUranium(IV) and Thorium(IV).Chapter Six Ligands Used to Prepare Metal Complexes.41 Trimethylphosphine.42 Tertiary Phosphines.43 Diphenylphosphine.44 Tri(phenyl-d3)phosphine.45 Methyl Difluorophosphite.46 Bi-, Tri-, and Tetradentate Phosphorus-Sulfur Ligands.47 Tetradentate Tripod Ligands Containing Nitrogen, Sulfur,Phosphorus, and Arsenic as Donor Atoms.48 Dimethyl(pentafluorophenyl)phosphine andDimethyl(pentafluorophenyl)arsine Ligands.49 Tris(?-dimethylarsinophenyl)arsine andTris(?-dimethylarsinophenyl)stibine.50 cis-2-Diphenylarsinovinyldiphenylphosphine and2-Diphenylarsinoethyldiphenylphosphine.51 [2-(Isopropylphenylphosphino)ethyl]diphenylphosphine.52 [(Phenylisopropylphosphino)methyl]diphenylphosphineSulfide.53N,N,N',N'-Tetrakis(diphenylphosphinomethyl)ethylenediamine.54 Ethylenebis(nitrilodimethylene)tetrakis(phenylphosphinicacid).55 [2-(Phenylphosphino)ethyl]diphenylphosphine.56 1,1,1-Trifluoro-4-mercapto-4-(2-thienyl)-3-buten-2-one.Chapter Seven Compounds of Biological Interest.57 Metalloporphyrins.58 (1,4,8,11-Tetraazacyclotetradecane)nickel(II) Perchlorate and1,4,8,11-Tetraazacyclotetradecane.59 N,N'-Ethylenebis(monothiacetylacetoniminato)cobalt(II)and Related Metal Complexes.60 Metallatranes.61cis-Bis(diethyldithiocarbamato)dinitrosylmolybdenum.62 Some ?-Cyclopentadienyl Complexes ofTitanium(III).Index of Contributors.Subject Index.Formula Index.
