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Full Description
Volumes in the Proven Synthetic Methods Series address the concerns many chemists have on irreproducibility of synthetic protocols, lack of identification and characterization data for new compounds, and inflated yields reported in chemical communications—trends that have recently become a serious problem. It is unique in that an independent checker has verified the experimental parts involved by repeating the protocols or using the methods. Featuring contributions from world-renowned experts and overseen by a highly respected series editor, this latest volume compiles reliable protocols for the preparation of intermediates for carbohydrate synthesis or other uses in the glycosciences.
Key Features:
Reliable and tested protocols for preparation of intermediates for carbohydrate synthesis
Offers a unique resource in glycosciences, compiling useful information in one reference
The protocols presented are of wide use to a broad range of readers in the carbohydrate field and the life sciences, including undergraduates taking carbohydrate workshops
Explores synthetic carbohydrate chemistry from both the academic and industrial points of view
The reader can be guaranteed a good clean reproducible experiment
Contents
Foreword. Preface. Guidelines for Authors. Remarks by the Series Editor. List of Contributors. About the Editors. About the Series Editor. Introduction. Chapter One: Preparation of N-Phenyltrifluoroacetimidoyl chloride (PTFAI-Cl) for the Synthesis of N-Phenyltrifluoroacetimidate (PTFAI) Donors. Chapter Two: Synthesis of α-D-Idose Pentaacetate from β-D-Glucose Pentaacetate via Paulsen Acetoxonium Rearrangement. Chapter Three: Synthesis of Methyl 2-deoxy-2-fluoro-α-D-mannofuranoside. Chapter Four: Phenyl 2-azido-2,3,6-trideoxy-3,6-difluoro-1-thio-α- and β-D-glucopyranoside. Chapter Five: Three-step Synthesis of Protected 1,6‑Di‑O‑acetyl‑D‑galactofuranoses. Chapter Six: Synthesis of Acyl β-C-glucosidic Compounds via Corey-Seebach Reaction. Chapter Seven: Synthesis of Ethyl α-Thioglycosides by Ethylation of α-Glycosyl Thiols. Chapter Eight: β-L-Rhamnosylation of p-Tolyl 2,3-di-O-benzoyl-4-O-benzyl-1-thio-β-D-glucopyranoside. Chapter Nine: Optimized Synthesis of Perbenzoylated Methyl 6,6',6''-triazido-6,6',6''-trideoxy-β-maltotrioside. Chapter Ten: Practical Synthesis of 2,6-Anhydro-4,5,7-tri-O-benzyl-1-deoxy-D-gluco-hept-1-enitol. Chapter Eleven: 3,4,6-Tri-O-benzyl-D-Glucal and 3,4,6-Tri-O-benzyl-D-Galactal. Chapter Twelve: Synthesis of 1,6-Anhydro-2-O-p-toluenesulfonyl-β-D-glucopyranose. Chapter Thirteen: Synthesis of 3-Chloropropyl 2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside. Chapter Fourteen: p-Tolyl 2,3,5-tri-O-acetyl-1-thio-β-D-xylofuranoside. Chapter Fifteen: 4,6-O-Benzylidene-2-O-levulinoyl-3-O-(2-naphthylmethyl)-β-D-glucopyranosyl Fluoride: A Crystalline and Versatile Building Block for Oligosaccharide Synthesis. Chapter Sixteen: Synthesis of Allyl 2-acetamido-2-deoxy-β-D-galactopyranoside. Chapter Seventeen: Synthesis of Orthogonally Protected p-Tolyl 2-azido-3-O-benzyl-6-O-tert-butyldiphenylsilyl-2-deoxy-4-O-levulinoyl-1-thio-β-D-glucopyranoside. Chapter Eighteen: Practical Synthesis of (1S)-1-Diethylphosphonomethyl-1,5-dideoxy-1,5-imino-D-xylitol: An Analogue of α-D-Glucose-1-phosphate. Chapter Nineteen: An Easy Synthesis of C-Glucosyl Chalcones and Dihydrochalcones. Chapter Twenty: Synthesis of Prop-2-ynyl 2-acetamido-6-O-tert-butyldiphenylsilyl-2-deoxy-β-D-glucopyranoside. Chapter Twenty-One: Synthesis of 3,4-Di[(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)oxy] benzaldehyde. Chapter Twenty-Two: Synthesis of Benzyl Protected NHPI Ester of Methyl D-Glucuronic Acid. Chapter Twenty-Three: Synthesis of 6-Bromo-6-deoxy-D-fructofuranose. Chapter Twenty-Four: Preparation of Gold Nanoparticles Decorated with Thiolated Galactosides. Chapter Twenty Five: 4-Bromophenyl 2,3,4-tri-O-acetyl-α-L-fucopyranoside. Chapter Twenty Six: Synthesis of Methyl 2-(4-[2,3,4,6-tetra-O-acetyl-α,β-D-galactopyranosyloxy]phenyl)acetate and Methyl 2-(4-[2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy]phenyl)acetate. Subject Index. Cumulative Author Index Vol 1-6.
