二次元NMR分光法を用いた有機構造決定(第2版)<br>Organic Structure Determination Using 2-D NMR Spectroscopy : A Problem-Based Approach (2ND)

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二次元NMR分光法を用いた有機構造決定(第2版)
Organic Structure Determination Using 2-D NMR Spectroscopy : A Problem-Based Approach (2ND)

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  • 製本 Paperback:紙装版/ペーパーバック版/ページ数 540 p.
  • 言語 ENG
  • 商品コード 9780123849700
  • DDC分類 541.22

基本説明

Key Features - Guides the reader in the practice of acquiring NMR data; Presents strategy for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra. The first edition of this book won the 2009 Choice Award for best chemistry publication in that year.

Full Description

Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach, Second Edition, is a primary text for a course in two-dimensional (2-D) nuclear magnetic resonance (NMR) techniques, with the goal to learn to identify organic molecular structure. It presents strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra.

The book begins with a discussion of the NMR technique, while subsequent chapters cover instrumental considerations; data collection, processing, and plotting; chemical shifts; symmetry and topicity; through-bond effects; and through-space effects. The book also covers molecular dynamics; strategies for assigning resonances to atoms within a molecule; strategies for elucidating unknown molecular structures; simple and complex assignment problems; and simple and complex unknown problems. Each chapter includes problems that will enable readers to test their understanding of the material discussed. The book contains 30 known and 30 unknown structure determination problems. It also features a supporting website from which instructors can download the structures of the unknowns in selected chapters, digital versions of all figures, and raw data sets for processing.

This book will stand as a single source to which instructors and students can go to obtain a comprehensive compendium of NMR problems of varying difficulty.

Contents

PART I: Background and Methods1. Introduction2. Instrumental Considerations3. Data Collection, Processing, and Plotting4. 1H and 13C Chemical Shifts5. Symmetry and Topicity6. Through-Bond Effects: Spin-Spin (J) Coupling7. Through-Space Effects: the Nuclear Overhauser Effect (NOE)8. Molecular Dynamics9. Strategies for Assigning Molecules10. Strategies for Elucidating Unknown Molecular Structures

PART II: Problems11. Simple Assignment Problems12. Complex Assignment Problems13. Simple Unknown Problems14. Complex Unknown Problems15. NMR Resonance Assignment Problems16. NMR Unknown Problems