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Full Description
Superbly organized and of great pedagogic value, 'Spectroscopy in Catalysis' describes the most important modern analytical techniques used to investigate catalytic surfaces. These include electron, ion, and vibrational spectroscopy, mass spectrometry, temperature-programmed techniques, diffraction, and microscopy. With the focus on practical use, rather than theory, each chapter presents current applications to illustrate the type of information that the technique provides and evaluates its possibilities and limitations, allowing selection of the best catalyst and the correct technique to solve a given problem.
This third edition includes significant new developments and case studies, with all the chapters updated by way of recent examples and relevant new literature. For students and for everyone who wants a digestible introduction to catalyst characterization.
From reviews of the previous editions:
'This is a truly valuable book ... very useful for industrial practitioners who need to be aware of the type of information that can be obtained from modern surface spectroscopies .... The book has a superb pedagogic value...'
Journal of Catalysis
'... this is an excellent text on spectroscopies in catalysis and I highly recommend it for ... introductory courses on heterogeneous catalysis or as a general introductory monograph.'
Journal of the American Chemical Society
Contents
INTRODUCTION
Heterogeneous Catalysis
The Aim of Catalyst Characterization
Spectroscopic Techniques
Research Strategies
TEMPERATURE-PROGRAMMED TECHNIQUES
Introduction
Temperature-Programmed Reduction
Temperature-Programmed Sulfidation
Temperature-Programmed Reaction Spectroscopy
Temperature-Programmed Desorption
Temperature-Programmed Reaction Spectroscopy in UHV
PHOTOEMISSION AND AUGER SPECTROSCOPY
Introduction
X-Ray Photoelectron Spectroscopy (XPS)
Ultraviolet Photoelectron Spectroscopy (UPS)
Auger Electron Spectroscopy
THE ION SPECTROSCOPIES
Introduction
Secondary Ion Mass Spectrometry (SIMS)
Secondary Neutral Mass Spectrometry (SNMS)
Ion Scattering: The Collision Process
Rutherford Backscattering Spectrometry (RBS)
Low-Energy Ion Scattering (LEIS)
MOESSBAUER SPECTROSCOPY
Introduction
The Moessbauer Effect
Moessbauer Spectroscopy
Moessbauer Spectroscopy in Catalyst Characterization
DIFFRACTION AND EXTENDED X-RAY ABSORPTION FINE STRUCTURE (EXAFS)
Introduction
X-Ray Diffraction
Low-Energy Electron Diffraction (LEED)
X-Ray Absorption Fine Structure (XAFS)
MICROSCOPY AND IMAGING
Introduction
Electron Microscopy
Field Emission Microscopy and Ion Microscopy
Scanning Probe Microscopy: AFM and STM
Other Imaging Techniques
VIBRATIONAL SPECTROSCOPY
Introduction
Theory of Molecular Vibrations
Infrared Spectroscopy
Sum-Frequency Generation
Raman Spectroscopy
Electron Energy Loss Spectroscopy (EELS)
CASE STUDIES IN CATALYST CHARACTERIZATION
Introduction
Supported Rhodium Catalysts
Alkali Promoters on Metal Surfaces
Cobalt-Molybdenum Sulfide Hydrodesulfurization Catalysts
Chromium Polymerization Catalysts
