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Full Description
This volume represents the proceedings of an international symposium on sample preparation, held at the University of Surrey, and jointly organised by the Chromatographic Society and the Robens Institute. The Chromatographic Society is the only international organisation devoted to the promotion of, and the exchange of information on, all aspects of chromatography and related techniques. With the introduction of gas chromatography in 1952, the Hydrocarbon Chemistry Panel of the Hydrocarbon Research Group of the Institute of Petroleum, recognising the potential of this new technique, set up a Committee under Dr S.F. Birch to organise a symposium on "Vapor Phase Chromatography" which was held in London in June 1956. Almost 400 delegates attended this meeting and success exceeded all expectation. It was to afford discussion of immediately apparent that there was a need for an organised forum development and application of the method and, by the end of the year, the Gas Chromatog raphy Discussion Group had been formed under the Chairmanship of Dr A.T. James with D.H. Desty as Secretary. Membership of this Group was originally by invitation only, but in deference to popular demand, the Group was opened to all willing to pay the modest sub scription of one guinea and in 1957 A.J.P. Martin, Nobel Laureate, was elected inaugural Chairman of the newly-expanded Discussion Group.
Contents
On-Line Sample Treatment for Column Liquid Chromatography.- Sample Preparation Using Supercritical Fluid Extraction.- (Post-Column) Reaction-Detection: An Alternative to Improve Sensitivity and Selectivity in Column Liquid Chromatographic Analysis.- Proton Nuclear Magnetic Spectroscopy: A Novel Method for the Study of Solid Phase Extraction.- The Effect of Cartridge Conditioning in the Reversed-Phase Extraction of Basic Drugs.- Experiences with Automated Sample Preparation in Bioanalysis.- Clinical Analysis from Biological Matrices.- A Rational Approach to the Development of Solid Phase Extraction Methods for Drugs in Biological Matrices.- The Analysis of Primary and Secondary Free Amino Acids in Biological Fluids: A Completely Automated Process Using On-Line Membrane Sample Preparation, Pre-Column Derivatisation with O-Phthalaldehyde, 9-Fluorenyl Methyl Chloroformate and High Performance Liquid Chromatographic Separations.- to Automated Sequential Trace Enrichment of Dialysates (ASTED) and Its Application to the Analysis of Nucleosides in Plasma.- High Resolution 1H NMR Spectroscopic Monitoring of Extraction of Model Glucuronides on Phenylboronic Acid and C18 Bonded Phases.- Solid Phase Extraction of the Highly Protein Bound Dopamine Uptake Inhibitor GBR 12909.- The Analysis of Valproic Acid in Human Plasma Using an Automated Sample Preparation Device (ASTED).- Problems and Solutions Encountered During Method Development for the Analysis of Nisoldipine, A Second Generation Calcium Antagonist.- The Use of Novel Bonded Phase Adsorbents for the Extraction of Drugs of Abuse from Biological Matrices.- Mixed Mode Solid Phase Extraction of Basic Drugs and their Metabolites from Horse Urine.- Aspects of Sample Preparation for Drug Analysis in Serum by Capillary Electrophoresis.- Strategical Considerations in Approaching Sample Preparations for Pesticide Residue Determination.- The Determination of Organochlorine Pesticides in Water.- Analysis of Pesticides and PCB Residues in Water, Soil and Plant Material.- Supercritical Fluid Extraction (SFE) — An Alternative to Traditional Techniques in Regulatory Environmental Analysis?.- Sampling and Analysis of Volatile Organics Using Automated Thermal Desorption.- Solid-Phase Extraction Procedure for the Assay of 1,4-Dioxane in Cosmetic Products.- Column Switching Strategies for Complex Petrochemical Sample Analysis.- Author Index.- Compound Index.
