Spectrochemical Analysis by X-Ray Fluorescence （1972）

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Spectrochemical Analysis by X-Ray Fluorescence （1972）

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  • 製本 Paperback:紙装版/ペーパーバック版／ページ数 326 p.
  • 言語 ENG
  • 商品コード 9781468417999
  • DDC分類 541

Full Description

In recent years the x-ray fluorescence technique has become increasingly important in modern analysis and production control; it can be classified as a spectroscopical method for the determination of the elemental com­ position. Many articles treat this method; however, there exists no modern textbook suitable for the beginner as well as the practician and theoretician. In this monograph the author intends to fill this need to present the prin­ ciples of x-ray fluorescence analysis and to develop a theoretical under­ standing of the technique. Both principles and theory w.ill be treated exten­ sively, for they are the basis for successful practical application of the method. X-ray fluorescence, on the other hand, is often carried out exclusively because of its practical usefulness. For this reason theoretical investigations are used exclusively as a basis for practical work and the multitude of applications, which constitute the value of the x-ray fluores­ cence method, will be explained on the basis of simple theory. The idea to write this monograph originated and developed when efforts to train coworkers required a more complete treatise. I would like to thank the elBA Aktiengesellschaft in Basel, where this work originated, for generous support and permission to publish the book. The head of the Physics Department, Dr. E. Ganz, and my colleagues have contributed to this book by providing a stimulating working atmosphere. I am grateful to my associates, in particular Messrs. E. Eng, S. Gasser, and H. R.

Contents

I Principles and Qualitative Analysis.- 1. Absorption and Scattering of X-Rays.- 2. Characteristic Emission Spectra.- 3. Photoelectrons, Fluorescent Yields, and Auger Electrons.- 4. Qualitative Analysis.- 5. Fluorescent Intensity of a Pure Element.- 6. Fluorescent Intensity of an Element in Two- and Multicomponent Mixtures.- 7. Interelemental or Secondary Excitation.- 8. Grain-Size and Surface Roughness Effects.- 9. Intensity Formula for a Divergent Primary Beam.- 10. Apparatus.- 11. Measurement Techniques.- II Quantitative Analysis.- 12. Calibration Curves and Regression Coefficients.- 13. Determination of Low Concentrations.- 14. Determination of Thin Film Thicknesses.- 15. Determination of High Concentrations with Calibration Curves.- 16. Determination of Concentration, Formulated as a Linear System of Equations.- 17. Analysis of Multicomponent Mixtures and Solutions for the Linear System of Equations.- III Examples of Applications and Abstracts.- 18. Analysis of Mixtures Which Are Difficult to Separate Chemically.- 19. Steel and Iron Industry.- 20. Base Metals and Ores.- 21. Light-Metal Industry.- 22. Determination of Thicknesses of Thin Films.- 23. Cement Industry and Silicate and Rock Chemistry.- 24. Petroleum and Coal Industry.- 25. Chemical Industry.- 26. Medicine and Biology.- 27. Analysis of Small Amounts of Substance and of Small Areas.- Text References and Articles Abstracted in Part III.