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This collection focuses on the characterization of minerals, metals, and materials as well as the application of characterization results on the processing of these materials. Focused sessions within the symposia include those centered on ferrous metals, non-ferrous metals, soft materials, ceramics, clays, composites, and minerals. In addition, sessions will focus exclusively on characterization concerns in the extraction, processing, and environmental application of materials. Finally, method development in characterization will be explored.
Contents
Preface xiii
About the Editorsxv
Characterization of Ceramics and Clays
FTIR and Raman Spectroscopic Investigation on the Structure of CaO-SiO2-TiO2 Ternary Slags 3
L. Wang, L. Wen, J. Tu, S. Zhang, and C. Bai
Characterization of Heavy Clay Ceramic Mixed with Red Mud Waste 11
C. Vieira, M. Babisk, U. da Silva Prado, and S. Monteiro
High-temperature Exposure of Oil Well Cements 17
B. Iverson, B. Waugh, and J. Maxson
Determination of Temperature and Time Calcination of Clays for Production of Metakaolin Based on Pozzolanic Activity 25
J. Alexandre, G. Xavier, A. Azevedo, S. Monteiro, and C. Vieira
PBT/Brazilian Clay Nanocomposites Prepared by Melt Intercalation: Effects of Organophilic Clay Content and Ionizing Radiation Treatment 33
M. Sartori, M. Ferreira, F. Díaz, V. Rangari, S. Jeelani, and E. Moura
Modification of Si3N4-SiC Heat Absorption Ceramic Material Using for Tower Type Solar Thermal Power Plant 45
M. Liu, X. Xu, J. Wu, G. Xu, G. Xue, and J. Liu
Microstructural and Electrical Properties of 0.5 mol% Al2O3-0.1 mol% B2O3-doped ZnO Ceramics 55
B. Yüksel and G. Hardal
Characterization of Composites
A Kinetic Analysis of a Thermal Curing Reaction of a Silicon Resin in Solid State 65
F. Vivier, D. Santamaria, D. Pellerej, P. Buonfico, and M. Sangermano
Halogen Free Flame Retardant for ABS Composite with Oxide Nanoparticles 73
P. Martins, T. Valera, J. Bartoli, and J. Tenorio
Investigation on the Thermal Conductivity of Resin Composite Materials 81
K. Monden
Polypropylene Nanocomposites Reinforced with Organophilic Clay and Brazilian Nut Fibers 89
L. da Rocha-Gomes, D. Fermino, E. Moura, M. Valenzuela, and F. Valenzuela-Diaz
Interfacial Evolution of Al/Cu Laminated Composite Produced by Asymmetrical Roll Bonding and Annealing 97
X. Li, G. Zu, and P. Wang
Characterization of Environmental Materials
Subsurface De-alloying during SCW Exposure 105
J. Li, Y. Zeng, O. Woo, W. Zheng, P. Liu, and C. Bibby
Characterization of Clay Brick Incorporated with Ash from the Incineration of Urban Garbage 113
N. Coutinho, S. Monteiro, and C. Vieira
Concrete of Steel Slag Composite for Paved Road and Its Hydration Microstructure 121
H. Fang, J. Hwang, G. Xue, L. Lu, and Y. Liu
Method for Removal of Mercury from Oil Field Brine with Calcium Carbonate Co-precipitation 131
F. Fazlollahi, M. Zarei, M. Habashi, and L. Baxter
Optical Parameters of Thermally Evaporated CdTe Thin Films 139
S. Ikhmayies
Obtaining the Polystyrene-bentonite Nanocomposite as a Method for Polystyrene Recycling 147
M. Machado, H. Wiebeck, F. Valenzuela-Diaz, M. Valenzuela, and V. Justo
Modified Hydrotalcites as Desulfurization Adsorbents: Preparation, Characterization, and Performance Test 157
A. Gomes, M. Mozumder, D. Cocke, T. Benson, H. McWhinney, and T. Grady
Thermal Analysis and Characterization of Elephant Grass Ash (Pennisetum Purupureums Shaum) Incorporated into Clay Matrix 165
R. Faria Jr., A. Silva, R. Toledo, S. Monteiro, and C. Vieira
Characterization of High-arsenic Sludge in Copper Metallurgy Plant 173
X. Zhu, X. Qi, H. Wang, Y. Shi, T. Liao, Y. Li, C. Liu, and X. Wang
Characterization of Ferrous Metals
In-Situ EBSD Investigation of Carbides during Annealing of AISI M42 Steel 187
M. Godec, B. Bati, and T. Pirtovsek
Effects of Heat Treatment on Transverse and Longitudinal Mechanical Properties of Engineering Machinery Steel WQ960 191
S. Tao, F. Wang, G. Sun, C. Li, and Q. Yan
Ultrasonic Non-Destructive Characterization of Power Plant Steel 199
M. El Rayes, E. El-Danaf, and A. Almajid
Study on Modification of Anti-oxidation Coating for Steel Billet 209
H. Chen, H. Gu, K. Lei, X. Chen, M. He, and G. Xue
Method Development in Characterization
Experimental Estimation of J Integral from Load-front Face Displacement Record for Compact Tension Specimens 219
K. Shi, L. Cai, Y. Hu, and D. Salmon
Structure Characterization of Sn-based and Ce-based Alloys Treated by Ultrafast Scanning 227
B. Zhao, L. Li, Q. Zhai, and Y. Gao
Anisotropic Finite Element Modeling of the Fused Deposition Modeling Process 235
S. Ogden and S. Kessler
Characterization of Material Processing
Characterization of Particle Damage and Surface Exposure of a Copper Ore Processed by Jaw Crusher, HPGR and Electro-dynamic Fragmentation 247
O. Gomes, D. de Oliveira, L. Sobral, and E. Pirard
Effect of Friction Stir Welding Speed and Post Weld Heat Treatment on the Microstructure and Hardness of AA7020 253
M. Ahmed, E. Ahmed, and A. Mahdy
Study on Reactivity between Mould Fluxes and High-Al Molten Steel 265
T. Wu, S. He, Y. Guo, and Q. Wang
Grinding Kinetics of Vanadium-titanium Magnetite Concentrate in a Ball Mill 271
R. Zhang, X. Lv, C. Ji, and X. Zheng
Arc Welding of Advanced High Strength Steels for Car-body Components 277
P. Spena, F. D'Aiuto, P. Matteis, and G. Scavino
Forging Hot and Cold: Development through the Ages 285
H. McQueen and E. Evangelista
Load Carrying Capacity and Microstructure of Resistance Spot Welded Dual-phase (DP600) Steel 297
S. Ataya
Optimization on Refining Slag and Tapping Deoxidation System for Carbon Structure Steel without Calcium Treatment 305
S. Zhao, Q. Wang, G. Chen, S. He, and M. Peng
Characterization in Material Extraction
Effects of Iron and Manganese Ions on Potentiostatic Current Transients for Copper Electrodeposition 315
A. Chen, J. Hwang, Z. Peng, Y. Ma, X. Liu, and X. Chen
Determination of Leaching Reaction Mechanism of Synthetic CaMoO4 in H2C2O4 Solutions 325
S. Ilhan, A. Kalpakli, and I. Yusufoglu
Effect of V2O3 and TiO2 on the Dissolution of Lime in FeO-SiO2-V2O3-TiO2 Slag 335
R. Tang, Y. Wang, S. Wang, B. Xie, and J. Diao
Characterization of Wastes Generated during Stainless Steel Production 343
X. Liu, J. Zhang, Q. Xiao, and Q. Li
Investigation of Reaction Stoichiometry of Leaching of Synthetic CaWO4 in H2C2O4 Solutions 351
A. Kalpakli, S. Ilhan, and I. Yusufoglu
Study on Extraction of Titanium from Titanium-bearing Blast Furnace Slags 361
Q. Xiao, J. Zhang, Y. Feng, and Q. Li
Characterization of Minerals
Microwave Permittivity, Permeability, and Penetration Depth of Pyrite 371
Z. Peng, J. Hwang, B. Kim, J. Kim, and X. Wang
Characterization of Waste from Ornamental Stones for Use in Mortar 379
A. Azevedo, J. Alexandre, G. Xavier, S. Monteiro, and C. Vieira
Titanomagnetite Properties and Microstructures 387
X. Liu, W. Schoenthal, T. Cox, A. Wise, D. Laughlin, and M. McHenry
Characterization of Clays Using for Formulations of Detergents 395
M. da Silva-Valenzuela, F. de Souza Carvalho, and F. Valenzuela-Diaz
Differential Characterization of Ikperejere Iron Shale and Iron Sandstone 401
O. Martin, O. Gerald, O. Kelechi, and B. Li
A New Process of Fluosilicic Acid Leaching for Recovering Bismuth from Materials Containing Bismuth Oxide 413
C. Zhang, X. Zhang, and J. Zhan
Fundamental Research on the Characteristics of Sierra Leone Iron Ore for Sintering 425
J. Dong, G. Wang, M. Zuo, H. Li, and Q. Xue
Characterization of Soft Materials I
Flexural Mechanical Characterization of Polyester Composites Reinforced with Continuous Banana Fibers 435
F. de Assis, F. Margem, R. Loiola, and S. Monteiro
Thermal Characterization of Epoxy Matrix Reinforced with Buriti Fibers by the Photoacoustic Technique 441
G. Altoe, F. Margem, S. Monteiro, R. Faria Jr., and T. Cordeiro
Characterization of Thermal Properties of Polyester Matrix Reinforced with Sisal Fibers by Photoacoustic Technique 449
A. Pereira, F. Margem, S. Monteiro, R. Faria Jr., and T. Cordeiro
Characterization of Thermal Properties of Curaua Fibers Incorporated in Epoxy Matrix by Photothermal and Photoacoustic Techniques 457
N. Simonassi, F. Margem, S. Monteiro, R. Faria Jr., and T. Cordeiro
Bending Tests in Polyester Composites Reinforced with Bamboo Fibers of the Specimen Dendrocalmus Giganteus 465
L. Martins, F. Margem, S. Monteiro, R. Loyola, and J. Margem
Characterization of Soft Materials II
Comparison between Bio-composite Based on Green HDPE/Brazil Nut Shell Fiber (BNSF) Treated and Non Treated by Electron-beam Radiation 475
R. Campos, M. Hosur, S. Jeelani, F. Diaz, E. Moura, and E. Seo
Dynamic-mechanical Behaviour of Epoxy Composites Reinforced with Jute Fiber 483
I. da Silva, A. Bevitori, C. de Oliveira, F. Margem, and S. Monteiro
Investigation on Mechanical and Morphological Behaviours of Copolyester/Starch Blend Reinforced with Rice Husk Ash 491
E. de Oliveira, V. Silva, R. Oliveira, A. Teran, A. Castillo, J. Harada, F. Diaz, and E. Moura
Charpy Toughness Behavior of Continuous Banana Fiber Reinforced Epoxy Matrix Composites 499
F. Assis, S. Monteiro, F. Margem, and R. Loiola
Thermal Photoacoustic Characterization of Polyester Composites Reinforced Ramie Fibers 507
C. de Oliveira, A. Bevitori, I. da Silva, F. Margem, G. Altoe, R. Faria Jr., T. Cordeiro, and S. Monteiro
Weibull Analysis of the Density of Ramie Fibers with Different Diameters 515
A. Bevitori, I. da Silva, C. de Oliveira, F. Margem, and S. Monteiro
Poster Session
Brazilian Bentonite Submitted to Mild Acid Treatment 525
C. Andrade, V. Justo, F. Mondelo, M. Valenzuela, C. Volzone, and F. Valenzuela-Diaz
Characterization of Different Clays for the Manufacture of Artifacts Ceramic Red 533
J. Alexandre, A. Azevedo, E. Zanelato, G. Xavier, S. Monteiro, and C. Vieira
Characterization of Laterite Nickel Ore 541
T. Li, X. Chen, B. Zhang, and X. Hong
Characterization of Sisal Fibers Thermal Properties by Photoacoustic Technique 549
A. Pereira, F. Margem, S. Monteiro, R. Faria Jr., and T. Cordeiro
Friction Stir Welding of Polycarbonate Sheets 555
M. Shazly, M. Ahmed, and M. El-Raey
In-Situ High Temperature X-ray Analysis of a Supermartensitic Stainless Steel 565
T. dos Santos, A. Rocha, R. de Carvalho, and V. Buono
Izod Impact Resistance of Jute Fiber Reinforced Polyester Matrix 573
I. da Silva, A. Bevitori, C. de Oliveira, F. Margem, and S. Monteiro
Izod Impact Tests of Polyester Composites Reinforced with Bamboo Fibers of the Specimen Dendrocalmus Giganteus 581
L. Martins, F. Margem, S. Monteiro, R. Loyola, and J. Margem
Obtaining Nanocapsules from PHBEG/MMT Composite 589
M. da Silva-Valenzuela, C. Matos, I. Sayeg, A. Moreira, H. Wiebeck, F. Valenzuela-Díaz, and W. Hui
Photoacoustic Characterization of Polyester Matrix Reinforced with Curaua Fibers 595
N. Simonassi, F. Margem, S. Monteiro, R. Faria Jr., and T. Cordeiro
Photoacoustic Thermal Characterization of Buriti Fibers 603
G. Altoe, F. Margem, S. Monteiro, R. Faria Jr., and T. Cordeiro
Preparation and Characterization of Polypropylene Nanocomposites with Organoclay and Discarded Bond 611
D. Fermino, M. Valenzuela, E. Moura, D. Parra, and F. Diaz
Research on Preparation and Properties of Inorganic Gelling Materials for Sand Fixation 619
M. He, J. Li, G. Xue, and F. Hao
Synthesis and Characterization of Ammonium Jarosite with Arsenic 627
F. Patino, M. Flores, I. Reyes, J. Mendez, M. Reyes, I. Mireles, and J. Hernandez
The Grain Growth Kinetics of 0.5 mol% B2O3-1 mol% TiO2-doped ZnO Ceramics 637
G. Hardal and B. Yüksel
Thermal Decomposition Reaction Mechanisms and Kinetics of Ammonium Paratungstate Tetrahydrate 645
A. Eser, C. Kahruman, and I. Yusufoglu
Author Index 655
Subject Index 659
