Techniques Labs for Macroscale and Microscale Organic Experiments （6TH）

Williamson, Kenneth/ Masters, Katherine M.

CENGAGE Learning Custom Publishing（2011/01発売）

• ページ数 336 p.
• 言語 ENG
• 商品コード 9781111430412
• DDC分類 540

Full Description

This manual derives many experiments and procedures from the classic Feiser lab text, giving it an unsurpassed reputation for solid, authoritative content. Featuring updated NMR spectra, new experiments that stress green chemistry and a Premium Website that includes glassware-specific videos with pre-lab, gradable exercises, this TECHNIQUES LABS edition of the authors' proven lab manual includes the most commonly used labs in the print manual and makes all the other experiments from MACROSCALE AND MICROSCALE ORGANIC EXPERIMENTS available for download on the companion website. Offering a flexible mix of macroscale and microscale options for most experiments, this proven manual emphasizes safety and allows users to save on the purchase and disposal of expensive, sometimes hazardous, organic chemicals. Macroscale versions can be used for less costly experiments, allowing users to get experience working with conventionally-sized glassware.

Contents

1. Introduction. 2. Laboratory Safety, Courtesy, and Waste Disposal. 3. Melting Points and Boiling Points. 4. Recrystallization. 5. Distillation. 6. Steam Distillation, Vacuum Distillation, and Sublimation. 7. Extraction. 8. Thin-Layer Chromatography: Analysis of Analgesics and Isolating Lycopene from Tomato Paste. 9. Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene, and Plant Pigments. 10. Gas Chromatography: Analysis of Alkene Isomers. 11. Infrared Spectroscopy. 12. Nuclear Magnetic Resonance Spectroscopy. 13. Mass Spectroscopy. 14. Ultraviolet Spectroscopy, Refractive Indices, and Qualitative Instrumental Organic Analysis. 15. Computational Chemistry.