In-Situ Spectroscopy of Monomer and Polymer Synthesis

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In-Situ Spectroscopy of Monomer and Polymer Synthesis

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  • 製本 Hardcover:ハードカバー版/ページ数 232 p.
  • 言語 ENG
  • 商品コード 9780306474101
  • DDC分類 547.28

Full Description


This book is a collection of selected papers presented at the symposium titled "In situ Spectroscopy in Monomer and Polymer Synthesis," held at the April, 2001 ACS National Meeting in San Diego, California, USA. The co-organizers of this symposium were Timothy Long, Judit E. Puskas, Robson F. Storey, and J. Andrews. In situ spectroscopic monitoring is gaining popularity both in academia and industry. FfIR monitoring is used most frequently, but UV-visible, raman, and NMR spectroscopy are also important. This book concentrates mostly on FfIR monitoring, both in the near and mid-infrared ranges. The first chapter is a short general overview of FfIR spectroscopy, followed by the symposium contribu- tions. We thought that this would be especially useful for student readers. We hope that the book will present a state-of-the-art overview of research related to in situ spectroscopic monitoring. -Judit E. Puskas ix Acknowledgments This book would not have been possible without the dedicated effort of the chapter contributors and the symposium committee: Professor Judit E. Puskas Professor Timothy Long Professor Robson F. Storey Professor J. Andrews The symposium was financially supported by: ACS-Petroleum Research Fund REMSPEC Co. Wyatt Technology Co.

Table of Contents

Introduction to Real Time Infrared                 1  (8)
Spectroscopic Monitoring
Sohel Shaikh
Sara van Zanden
Judit E. Puskas
The Allure of ``Molecular Videos'': In situ 9 (28)
Infrared Spectroscopy of Polymerization
Processes
A. J. Pasquale
J. R. Lizotte
D. T. Williamson
T. E. Long
Real-time Fiber Optic Monitoring of 37 (22)
Solution and Suspension Polymerization
Processes
Judit E. Puskas
Armin J. Michel
L. Bryan Brister
Eraclis Tzaras
Gregory Marr
Monika Hoffman
Karin Weiss
Investigation of High Temperature, 59 (8)
Isobutylene Polymerizations Utilizing
Real-Time ATR-FTIR Spectroscopy
Casey D. Stokes
Robson F. Storey
Application of FT-NIR Spectroscopy for 67 (16)
Monitoring the Kinetics of Living
Polymerizations
M. G. Lanzendorfer
H. Schmalz
V. Abetz
A. H. E. Muller
Spectroscopic Techniques for Continuous 83 (26)
Monitoring of Emulsion Polymerization
Reactions
A. M. Cardenas-Valencia
V. Shastry
L. H. Garcia-Rubio
Kinetic Study of Photoinitiated 109(16)
Polymerization Reactions by Real-Time
Infrared Spectroscopy
Christian Decker
Frederic Masson
Catherine Bianchi
In Situ NMR Monitoring of Living Radical 125(22)
Polymerization
Sebastien Perrier
David M. Haddleton
Real-Time Monitoring of Isocyanate 147(16)
Chemistry Using a Fiber-Optic FTIR Probe
Mary A. Thomson
Peter J. Melling
Real-Time Monitoring of the Componnets in 163(10)
PVC Melt Compounds Using NIR Spectroscopy
during Extrusion
D. Fischer
In Situ Analysis of the Thermal Elimination 173(14)
Reaction in the Synthesis of
Poly(p-phenylene vinylene) (PPV) and PPV
Derivatives
Georgia A. Arbuckle-Keil
Yolanda Liszewski
James Wilking
Bing Hsieh
Carbonylation of Methanol over Supported 187(20)
Rhodium Catalysts
Jeno Bodis
Index 207