有機化学における高解像度NMR手法（第３版） High-Resolution NMR Techniques in Organic Chemistry （3RD）

Claridge, Timothy D.W.

Elsevier Science Ltd（2016/05発売）

Elsevier Science Ltd（2016/05発売）

• 製本 Paperback:紙装版/ペーパーバック版／ページ数 552 p.
• 言語 ENG
• 商品コード 9780080999869
• DDC分類 543.66

Full Description

High-Resolution NMR Techniques in Organic Chemistry, Third Edition describes the most important NMR spectroscopy techniques for the structure elucidation of organic molecules and the investigation of their behaviour in solution. Appropriate for advanced undergraduate and graduate students, research chemists and NMR facility managers, this thorough revision covers practical aspects of NMR techniques and instrumentation, data collection, and spectrum interpretation. It describes all major classes of one- and two-dimensional NMR experiments including homonuclear and heteronuclear correlations, the nuclear Overhauser effect, diffusion measurements, and techniques for studying protein-ligand interactions. A trusted authority on this critical expertise, High-Resolution NMR Techniques in Organic Chemistry, Third Edition is an essential resource for every chemist and NMR spectroscopist.

Contents

1. Introduction
2. Introducing High-Resolution NMR
3. Practical Aspects of High-Resolution NMR
4. One-Dimensional Techniques
5. Introducing Two-Dimensional and Pulsed Field Gradient NMR
6. Correlations Through the Chemical Bond I: Homonuclear Shift Correlation
7. Correlations Through the Chemical Bond II: Heteronuclear Shift Correlation
8. Separating Shifts and Couplings: J-Resolved and Pure Shift Spectroscopy
9. Correlations Through Space: The Nuclear Overhauser Effect
10. Diffusion NMR Spectroscopy
11. Protein-Ligand Screening by NMR
12. Experimental Methods
13. Structure Elucidation and Spectrum Assignment